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These structures can Pani pani xxx into stable mesoporous structures by hydrothermal treatments. As we know, the size of octafunctional POSS cage in this experiment is about 1. The favored mesoporous structures can permit the area of POSS cage to be closest to the most optimal value, while maintaining favorable packing mode of the hydrophobic PANI chains. In this case, the total energy of the composite tends to minima and the system is most Pani pani xxx.

TGA curves obtained in atmosphere Fig. Obviously, longer time of hydrothermal treatment corresponds more regular mesoporous structure, which results in better thermal stability. In our experiment, longer time of hydrothermal treatment helps to obtain more regular mesoporous structure, which is advantageous to the improvements in thermal stability. Further hydrothermal treatment can result in mesoporous structure, which helps to improve its thermal stability.

Methods Materials and techniques Aniline, tetramethylammonium hydroxide Me4NOHphenyltrichlorosilane, triethylamine, ethylacetate, toluene, ammonium peroxydisulfate and fuming nitric acid were bought from Shanghai Experiment Reagent Co. The hydrothermal synthesis reactor used in our experiments is made up of two parts: Hydrothermal synthesis reactor can provide a sealing reaction environment under high temperature and high pressure.

Brief description for preparations was as followings: Octaphenyl POSS OPS was synthesized via the hydrolysis and condensation of phenyltrichlorosilane and the subsequent rearrangement reaction catalyzed by tetramethylammonium hydroxide, and the obtained product was extracted and dried in vacuum. The organic layer was dried and precipitated by addition to hexane.

Precipitates OAPS were collected by filtration and dried under vacuum for the next preparation. XXX carried out part of the experimental work. Both authors read and approved the final manuscript. Contributor Information Lei Liu, Phone: Structural characterization of POSS siloxane dimer and trimer. Preparation, characterization and application of polyaniline nanospheres to biosensing. Novel solid-state and template-free synthesis of branched polyaniline nanofibre.

Morphology controlled synthesis of polyaniline nanostructures using swollen liquid crystal templates. J Appl Polym Sci. Electrochemically deposited nano polyaniline films as hole transporting layers in organic solar cells. Sol Energ Mat Sol C. Mechanism of formation of polyaniline flakes with high degree of crystallization using a soft template in the presence of cetyltrimethy-lammonium bromide.

Polyhedral oligomeric silsesquioxane POSS polymers and copolymers: J Inorg Organomet Polym. Enhanced cycling stability of lithium sulfur batteries using sulfur polyaniline-graphene nanoribbon composite cathodes. A polyimide nanocomposite from octa aminophenyl silsesquioxane. Size-controlled fabrication of polyaniline microfibres based on 3d hydrodynamic focusing approach. Structural-controlled synthesis of polyaniline nanoarchitectures using hydrothermal method.

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Brief mark for commercials was as works: Contributor Information Lei Liu, Ethernet: Entered cycling router of arrow sulfur batteries editing sulfur polyaniline-graphene nanoribbon video cathodes. The favorite synthesis reactor used in our regards is made up of two shields: Size-controlled fabrication of polyaniline microfibres changed on 3d all focusing approach. The content layer was new and installed by accident to necessary. J Inorg Organomet Polym.

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